BAC Analysis Utilizing GCMS and FID Combined with Fully Automated Sample Prep Performed by Robotic Sampler

Blood Alcohol Content (BAC) analysis by gas chromatography (GC) and gas chromatography/mass spectrometry (GCMS) is a standard analytical technique that has been around for years. However, the standard and sample prep is laborious and tedious. Using a custom script and robotic autosampler with syringe swap capability, a protocol was developed to automatically prepare calibration and check standards, perform internal standard addition, and perform headspace (HS) injections into a GCMS paired with FID establishing a turn key system for BAC analysis.
In this study, the quantitative accuracy and reproducibility of four analytes were tested with a Shimadzu GCMS/FID with AOC-6000 multifunction robotic autosampler.

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Gas Chromatography, Gas Chromatograph-Mass Spectrometry, Mass Spectrometry
Blood Alcohol Content, Pharmaceutical, Life Science, AOC-6000
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