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User Benefits Application News Introduction Carbon fiber reinforced plastic (CFRP) has high specific strength and stiffness and is widely used in various industrial fields, including transport vehicles. In order to ascertain its long-term reliability and durability as a structural material, it is necessary to evaluate it for fatigue, one of the main causes of structural failure. However, since CFRP is composed of two types of materials, carbon fibers and matrix resin, it exhibits complex behaviors in failure, such as matrix cracking, inter-layer delamination, and fiber rupture. This article describes bending fatigue tests that used the Servopulser EHF-L tabletop dynamic and fatigue testing system. The extension of cracks during the fatigue tests was observed using the SEM Servopulser, a high-temperature fatigue testing machine with a scanning electron microscope. Test Specimen Information and Measurement System The test specimen information is shown in Table 1. The EHF-L and the SEM Servopulser were used in the tests. The test equipment configuration is shown in Table 2. First, the CFRP test specimen S- N curve was created using the EHF-L. Then, the fatigue testing conditions were set on the SEM Servopulser based on the S-N curve obtained, and the cracking process was observed. The SEM Servopulser can perform three-point bending fatigue tests of carbon fiber reinforced plastic. The SEM Servopulser can also be used to observe fatigue cracks. High-accuracy dynamic control can be achieved with the Servo Controller 4830. Three-Point Bending Fatigue Tests of Carbon Fiber Reinforced Plastic Using the SEM Servopulser Fumiaki Yano and Yuki Nishikawa Tabletop Dynamic and Fatigue Testing System Servopulser EHF-L Series High-Temperature Fatigue Testing Machine with Scanning Electron Microscope SEM Servopulser Table 1 Test Specimen Information Table 2 Equipment Configuration Static Three-Point Bending Test Results To set the conditions in the fatigue tests, static three-point bending tests were performed. The test conditions are shown in Table 3, and the stress-displacement curves are shown in Fig. 1. The mean value of the flexural strength in the static three-point bending tests was 628 MPa (standard deviation 50.6 and coefficient of variation 8.1). The loading conditions in the fatigue tests were based on this value. The test setup is shown in Fig. 2. Table 3 Test Conditions Fig. 2 Test Setup Fig. 1 Stress - Displacement Curves Stress [MPa] Displacement [mm] Test Specimen: CFRP Lamination Method: (0/90)/(45/-45) alternate lamination Dimensions: Length 36 × width 5 × thickness 3 mm Testing Machine: EHF-L, SEM Servopulser Load Cell: 10 kN Test Jig: Three-point bending test jig Control Device: Servo Controller 4830 Software: Windows software for 4830 Test Speed: 1 mm/min Number of Tests: n = 4 Distance between Supports: 30 mm Indenter/Support Point: R2 Apparatus Used: EHF-L
Application News Three-Point Bending Fatigue Test Results The loading conditions in the three-point fatigue tests were 60 to 85 % of the static three-point flexural strength. The test conditions are shown in Table 4, and the S-N curves are shown in Fig. 3. Fig. 5 Examples of Observations Using the SEM Servopulser (1) Before the test (2) 719 cycles, magnification ×30 (3) 719 cycles, magnification ×50 (4) 719 cycles, magnification ×100 (5) 5,500 cycles, magnification ×13 (6) 5,500 cycles, magnification ×100 Table 4 Three-Point Bending Fatigue Test Conditions Observations Using the SEM Servopulser The SEM Servopulser combines a scanning electron microscope (SEM) with a fatigue testing machine (Servopulser). This enables the extension of cracks to be observed in detail during tests. From the S-N curve in Fig. 3, observations using the SEM Servopulser were performed up to a maximum loading stress of 535 MPa. Fig. 4 shows a photograph of the test specimen and test jig. To make the test specimen more easily observed using the SEM, the test specimen was coated with gold in advance. Fig. 5 shows images observed using the SEM Servopulser. Fig. 5 (1) shows the test specimen directly below the indenter before the test. Fig. 5 (2) to (4) show the test specimen close to the indenter when the number of cycles was 719. The SEM magnification ratio was 30, 50, and 100, respectively. From Fig. 5 (2) to (4), compression failure, including the rupture of fibers, was observed on the left side of the indenter. Fig. 5 (5) and (6) show the test specimen when the number of cycles was 5500 with a magnification ratio of 13 and 100, respectively. From Fig. 5 (5), it can be seen that cracking occurred not only on the indenter side but also on the opposite side. In Fig. 5 (6), a new matrix crack that was not observed in Fig. 5 (4) was observed, so it is clear that the damage had progressed. Fig. 4 Test Specimen and Test Jig Indenter Specimen Support point Support point Fig. 3 S-N Curve Note: Each blue point is one fatigue test result. The point with an arrow indicates that even at the prescribed number of cycles (10 million) the specimen did not fail Max. Loading Stress [MPa] Number of Cycles to Failure [Cycles] Maximum Loading Stress: 377, 409, 440, 472, 503, 535 [MPa] (60 to 85 % of the static flexural strength) Stress Ratio: 0.1 Frequency: 20 Hz Number of Tests: n = 2 Distance between Supports: 30 mm Indenter/Support Point: R2 Apparatus Used: EHF-L (1) (2) (3) (4) (5) (6) Indenter Specimen
Application News www.shimadzu.com/an/ Shimadzu Corporation © Shimadzu Corporation, 2024 For Research Use Only. Not for use in diagnostic procedures. This publication may contain references to products that are not available in your country. Please contact us to check the availability of these products in your country. The content of this publication shall not be reproduced, altered or sold for any commercial purpose without the written approval of Shimadzu. See http://www.shimadzu.com/about/trademarks/index.html for details. Third party trademarks and trade names may be used in this publication to refer to either the entities or their products/services, whether or not they are used with trademark symbol “TM” or “”. Shimadzu disclaims any proprietary interest in trademarks and trade names other than its own. The information contained herein is provided to you "as is" without warranty of any kind including without limitation warranties as to its accuracy or completeness. Shimadzu does not assume any responsibility or liability for any damage, whether direct or indirect, relating to the use of this publication. This publication is based upon the information available to Shimadzu on or before the date of publication, and subject to change without notice. Servopulser is a trademark of Shimadzu Corporation or its affiliated companies in Japan and/or other countries. Conclusion Bending fatigue tests were performed on CFRP using a fatigue testing system, and the resulting S-N curve was compiled. Then the conditions were set on the SEM Servopulser based on the S- N curve obtained, and damage to the test specimen was observed during the test. By changing the magnification on the SEM, it was possible to observe the damage location on the test specimen in detail. As the test progressed, it was possible to clearly observe how the damage progressed. In this way, the SEM Servopulser demonstrated it can assist in evaluating the fatigue properties of composite materials, such as CFRP. Related Applications 1. Three-Point Bending Fatigue Test and Crack Observation of Cracked Specimens Using SEM Servopulser Application News No. 01-00794 2. Three-Point Bending Fatigue Tests of Welded Material Using the SEM Servopulser Application News No. 01-00792 First Edition: Nov. 2024 01-00793-EN
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