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User Benefits Application News Fig. 1 Dynamic and Fatigue Testing System Servopulser EHF-L Measurement System Table 1 shows the instrument configuration. A tabletop dynamic and fatigue testing system, Servopulser EHF-L, was used in this test (Fig. 1). Table 2 shows the test specimen information. Rigid PVC and PC were used in this test. The test setup is shown in Fig. 2. It is widely known that the mechanical properties of plastic materials are temperature- dependent. 1) In addition, during a fatigue test, the temperature may rise due to the heat generated by the specimen. This phenomenon depends on the material properties, and tends to become more pronounced as the frequency and applied stress increase. Therefore, in this test, the surface temperature of the specimen was measured using a radiation thermometer, and the frequency of the fatigue test was set so that the specimen temperature would be 30 °C or less. For the temperature measurement, blackbody paint was applied to the center of the specimen. Additionally, a prototype jig with improved operability was used for this measurement. Table 1 Instrument Configuration Introduction Plastic materials are widely used in daily necessities such as PET bottles due to their light weight, low cost, superior moldability, and colorability. In recent years, in addition to general-purpose plastics such as polyvinyl chloride (PVC) and polyethylene (PE), engineering plastics with improved heat resistance and mechanical strength such as polycarbonate (PC) and polyamide (PA) have attracted attention. These materials are used as structural materials and mechanical components in automobiles, aircraft, and piping, and are increasingly used in applications that require performance in particularly harsh environments. In the process leading to the failure of a material, even a small load such as vibration that does not break a material with a single load can cause failure due to repeated action. This phenomenon is called “fatigue.” Because plastic materials used as structural materials are expected to be subjected to repeated loads over a long period of time, evaluation of fatigue characteristics is essential for product safety. This article introduces an example of fatigue testing of plastics in accordance with JIS K 7118. It is possible to test in accordance with JIS K 7118 “General rules for testing fatigue of rigid plastics” by using the dynamic and fatigue testing system Servopulser, EHF-L Series. High-accuracy dynamic control can be achieved with Servo Controller 4830. The surface temperature of the test specimen can be measured in real time, and the collected data can be incorporated into the control system. Fatigue Testing of Rigid Plastics (JIS K 7118) Tsubasa Yamamoto and Fumiaki Yano Tabletop Dynamic and Fatigue Testing System Servopulser EHF-L Series Specimen Radiation thermometer Prototype jig Static Test Results Static tensile tests were performed to set the fatigue test conditions. Table 3 shows the test conditions for the static tensile tests. Fig. 3 shows the stress-strain diagram for each specimen. Table 4 shows the ultimate tensile strength of each specimen from the static test results. Testing Machine: Servopulser EHF-LV20k1A Load Cell: 5 kN Actuator Stroke: ±25 mm Control Unit: Servo Controller 4830 Software: Windows Software for 4830 Test Jig: Non-shift screw-type grips (prototype) Thermometer: Radiation Thermometer FT-H10 (KEYENCE) Fig. 2 View of the Test Table 3 Static Test Conditions Test Speed: 50 mm/min Number of Specimens: n = 3 Material Properties: Rigid polyvinyl chloride (PVC) Polycarbonate (PC) Shape: ISO527-2-1A (JIS K 7161-2-1A) Dimensions of the Parallel Section: W10 × t4 × L80 mm Table 2 Test Specimen Specimen Static Ultimate Tensile Strength [MPa] Standard Deviation Coefficient of Variation (CV) Rigid PVC 74.70 0.059 0.001 PC 64.05 0.118 0.002 Table 4 Static Test Results
Application News www.shimadzu.com/an/ Shimadzu Corporation © Shimadzu Corporation, 2025 For Research Use Only. Not for use in diagnostic procedures. This publication may contain references to products that are not available in your country. Please contact us to check the availability of these products in your country. The content of this publication shall not be reproduced, altered or sold for any commercial purpose without the written approval of Shimadzu. See https://www.shimadzu.com/about/trademarks/index.html for details. Third party trademarks and trade names may be used in this publication to refer to either the entities or their products/services, whether or not they are used with trademark symbol “TM” or “”. Shimadzu disclaims any proprietary interest in trademarks and trade names other than its own. The information contained herein is provided to you "as is" without warranty of any kind including without limitation warranties as to its accuracy or completeness. Shimadzu does not assume any responsibility or liability for any damage, whether direct or indirect, relating to the use of this publication. This publication is based upon the information available to Shimadzu on or before the date of publication, and subject to change without notice. PC First Edition: Sep. 2025 01-00917-EN Servopulser is a trademark of Shimadzu Corporation or its affiliated companies in Japan and/or other countries. Fatigue Test Results Table 5 shows the fatigue test conditions. Six conditions were set for the maximum loading stress in the fatigue tests: from 20 to 70 % of the ultimate tensile strength in the static test results. Fig. 4 shows the relationship between the maximum loading stress and the specimen temperature. This time, the test was conducted with the frequency determined so that the surface temperature was 30 °C or less. Although the surface temperature of the specimen increased as the maximum loading stress increased, it can be confirmed from Fig. 4 that the tests were conducted at 30 °C or less. Fig. 5 shows the relationship between the maximum loading stress and the number of cycles to failure (S-N diagram). In this article, S-N diagrams were obtained for two types of materials and it was possible to evaluate their fatigue properties. Conclusion In these tests, rigid PVC and PC were subjected to fatigue tests in accordance with JIS K 7118 using the dynamic fatigue testing machine Servopulser EHF-L. The surface temperature of the specimens was measured using a radiation thermometer. As described above, this instrument configuration can be used for fatigue characterization of plastic materials. <References> 1) Takeshi Kunio: Materials System, 6 (1987), 7-19 Maximum Loading Stress: The percentages of static ultimate tensile strength were as follows PVC 20, 30, 40, 50, 60 % PC 20, 30, 40, 50, 60, 70 % Stress Ratio: 0.1 Maximum Cycles: 1.0 × 10 6 Cycles Frequency: 5 Hz Number of Specimens: n = 2 Test Temperature: 23 °C Table 2 Fatigue Test Conditions 0 10 20 30 40 50 60 70 0 10 20 30 Stress [MPa] Strain [%] 0 10 20 30 40 50 60 70 80 0 2 4 6 8 Stress [MPa] Strain [%] 20 21 22 23 24 25 26 27 28 29 30 20 30 40 50 Surface Temperature of Specimen [°C] Maximum Loading Stress [MPa] 20 22 24 26 28 30 10 20 30 40 50 Surface Temperature of Specimen [°C] Maximum Loading Stress [MPa] 0 10 20 30 40 50 60 70 80 1.E+03 1.E+04 1.E+05 1.E+06 1.E+07 Maximum Loading Stress [MPa] Number of Cycles to Failure 2 points 0 10 20 30 40 50 60 70 80 1.E+03 1.E+04 1.E+05 1.E+06 1.E+07 Maximum Loading Stress [MPa] Number of Cycles to Failure (a) (b) (a) (b) Rigid PVC PC Fig. 3 Stress-Strain Curves (a) Rigid PVC, (b) PC Rigid PVC PC Rigid PVC Fig. 5 S-N Diagram (a) Rigid PVC, (b) PC Fig. 4 Surface Temperature of Specimen-Maximum Load Stress Curves (a) Rigid PVC, (b) PC (a) (b)
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