Automatic Derivatization System for Phenethylamine Drugs - Applications

Applicable to GCMS-QP2050, GCMS NX series

Add Bookmark

{"title":"Applications","columnTitle":"Applications","source":"product","key":3281,"filter_types":["applications","application_note","posters"],"config_list":[],"anchor":"table_anchor_applications","filter":true} {"title":"Technical Documents","columnTitle":"Technical Documents","source":"product","key":3281,"filter_types":["technical","technical_reports","white_papers","primers"],"config_list":[],"anchor":"table_anchor_technical","filter":true} {"title":"Manuals","columnTitle":"Manuals","source":"product","key":3281,"filter_types":["manuals"],"config_list":[],"anchor":"table_anchor_manual","filter":true}
adobe

Most of the documents on the LITERATURE is available in PDF format. You will need Adobe Acrobat Reader to open and read PDF documents. If you do not already have Acrobat Reader, you can download it free at the Adobe's Website. Click the GET ADOBE READER icon on the left to download a free copy of Adobe Acrobat Reader.

Application to Authentic Samples Using Automatic On-column Derivatization System

  • An authentic urine sample was pretreated using the liquid-liquid extraction shown in Fig. 1. TFA derivatives of methamphetamine and amphetamine were detected in the urine samples.　These results demonstrate the ability of qualitative and quantitative analysis using 2-step injection with high selectivity in authentic samples.

  • sample-pretreatment-flow.


    Fig.1 Sample pretreatment flow

Total Ion Current Chromatograms (TICC) of authentic urine sample
 

Fig. 2 Total ion current chromatograms (TICC) of authentic urine sample

Mass Chromatograms of Detected Drugs
 

Fig. 3 Mass chromatograms of detected drugs