User interviews December 2020
Our field of activity is contract research and testing for life sciences industries including pharma, biotech, nutraceuticals, environmental sciences, food&agri testing, and diagnostics.
LC/MS/MS Method Package for Residual Pesticide Ver. 3
For LabSolutions™ LCMS Software
- ■ Database compatible with LabSolutions Connect, a tool that automates MRM tuning and optimization
- Encompasses the components listed in the Japanese Multiresidue Method for Agricultural Chemicals by LC/MS.
- Compatible with the components subject to the Chinese GB standards
- Compatible with the components subject to (EC) Directive No. 396/2005
- Contains 6557 MRM transitions for 836 components.
- ■ Pretreatment program for improving the peak shape of polar pesticides
- ■ Easy data analysis with LabSolutions Insight, a powerful data mining and analytics program
Create Methods Easily from the Database
The MRM information in this method package is controlled by LabSolutions Connect (option). With LabSolutions Connect, you can call up the information needed from the database by loading a text file, and then easily create an analysis method. In addition, this method package contains text files (search lists) of components subject to the regulations, enabling the easy creation of an analysis method file for these components.
The database and search lists can be customized for use in conjunction with components to be analyzed by the user.
Improve the Shape of Peaks for Polar Compounds via Co-Injection
Co-Injection of Water Using the Pretreatment Mode in the SIL-30AC Autosampler
MRM Chromatograms for Pesticides Added to a Tomato Extract (Sample injection volume: 2 μL)
Samples pretreated with the QuEChERS method are extracted with 100 % acetonitrile. Accordingly, the shape of peaks for polar compounds with short retention times is prone to deformation depending on the analytical conditions (figure at right (1)).
A pretreatment program for co-injection is incorporated into the high-speed simultaneous analysis methods for 508 and 646 residual pesticides. Reducing peak shape deformation is possible by co-injecting water with the sample (figure at right (2)).
Note: The co-injection mode is supported only by the SIL-30AC.
Smooth Analysis of Multiple Analytes with LabSolutions Insight
When analyzing data for multiple components and analytes, everything from batch analysis to the creation of reports can be performed by LabSolutions Insight.
LabSolutions Insight is a software program equipped with quantitative analysis and screening functions. In the analysis window, information is displayed for each target compound and set of measurement data, and both quantitative values and area values can be listed. This allows the user to select the easiest display method for checking the data in accordance with the workflow.
In addition, by using the flagging function, only the results exceeding specified standard values are displayed, improving the analytical throughput of multiple components and analytes subject to the regulations.
Precaution
LabSolutions LCMS Ver. 5.86 or later is required.
News / Events
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LCMS Food Safety Application is now available.
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Application Note: "Analysis of Pharmaceuticals' Impurity - Regulations and Analysis for Carcinogenic Substances -"
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Application Note: "Various Analysis Techniques for Organic Acids and Examples of Their Application"
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Shimadzu has released the Metabolites Method Package Suite.
Provides ready-to-use methods for over 1900 metabolites
This suite allows comprehensive analysis of over 1900 metabolites without the need for investigation of separation conditions, MRM optimization or parameter settings. -
Direct Probe Ionization Mass Spectrometer - APPLICATION NOTEBOOK -
Sustainability initiatives
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2 Zero hunger
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6 Clean water and sanitation